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The focus will be on determining crucial factors that might affect the method. 761 0 obj <>stream At room temperature polyethylene oxide is miscible with water in all proportions. 5 0 obj<>stream uuid:38bb500f-f0d5-4fbc-906f-f0051166d996 The similarities to USP Apparatus II (same vessel as the rotating disk but a paddle The information is provided for those who use, prepare, and dispense drugs, solely to indicate descriptive and solubility properties of … h�b```f``�``g`�bd@ AV ��a8qo�Pl�_�� �]\�R|�[,$�ݴ� {�4�sחM����fz0ZJjfo���97�t ל�7./Y(�q]��h�����w�:��V�T���u��-a�v�Gǰttt4Ht4t40w���B1�( ,٠R����vc ��]����X�BS~F�'�!V5�;���p�Qnw�6�(���+�!�����!щq��;�1V3p�1��H�1p�?��u �e� �� E���a��ay��d�$�*0z���\�I[ �Ea�B��7B5W���?FI��#�W+��8���F�1���M�0�(�$�(. 7 0 obj <> endobj h�bbd```b``��� �q?�d}"Y��l�`�N0{X�-�]_f����Ȓ* ���v]"E�A$W+Xo��?ӏ����)l/#M��: pS Trace impurities may affect solubility greatly. [�A��2��@����a9����WF��}�K��0�s���f��Y5�v����Y#���{N��P@�7�y�@S����K;k�o�H���#ua��o�-��K*�};J?#:O%�jދo���c�9���N�� The “description” and “solubility” statements pertaining to an article (formerly included in the individual monograph) are general in nature. 135 A study report should be created after the experiment detailing the actual experimental conditions, 136 results (raw data plus mean values with standard deviations) and any observations such as, for 137 example, the degradation of an API due to pH or buffer composition. %PDF-1.4 744 0 obj <>/Filter/FlateDecode/ID[<9CA933CE75B1004B90901D9CCEF07966><4B95935A2AE6D24DAFF513C4EEF8DE35>]/Index[724 38]/Info 723 0 R/Length 104/Prev 510855/Root 725 0 R/Size 762/Type/XRef/W[1 3 1]>>stream 3 0 obj<> endobj pKa – 1, and at pH = 1 and 7.5. Pharmacopeial area and a make a pre-study of the rotating disc. 2 0 obj<> endobj Allow to stand for 24 h. ... SOLUBILITY For this test a maximum of 111 mg of substance (for each solvent) and a maximum of 30 ml of each solvent are necessary. Information about an article's “description and solubility” also is provided in the reference table Description and Relative Solubility of USP and NF Articles. 14 0 obj<> endobj Apparatus * Constant-Temperature Bath— Use a constant-temperature bath that is capable of maintaining the temperature within ±0.1 and that is equipped with a horizontal shaft capable of rotating at approximately 25 rpm. endstream endobj 5350Description and Solubility / Reference Tables First Supplement to USP 35–NF 30 DESCRIPTION AND SOLUBILITY Description and Relative Solubility of USP and NF Articles The “description” and “solubility” statements pertainingand other particulate matter, unless limited or excluded by 10 0 obj/Encoding<>>>>> endobj 16 0 obj[/Indexed/DeviceRGB 253 28 0 R] endobj 4 0 obj<> endobj p�m�g�;F=PR�����(&���e6MW�����*��[)I���_I�i� �_6�T��Ĵ?�� qDE�l�i ��ߏ@�o���U2=`��s���W��R B@���odñ���J��$!k�^�E!K�xu�������,rb���s#���E>Sr0�ғ`�xJVF�=a�7��z+�r�Q�Š��$C�6[Bg�9�Z X�5B>S%�t��x�C�ySӂ��%�3_�E�k� ���J�. SOLUBILITY For this test a maximum of 111 mg of substance (for each solvent) and a maximum of 30 ml of each solvent are necessary. The water solubility, hygroscopicity, solubility in organic solvents, and melting point do not vary in the specified molecular weight range. �1WI����9>�_R"d��IJ�%�!`�JiHh=`C�}H�"��E�(d�Y��w �Էd] d��M���=C�� 6�aL$�(GB)8�aoʼn�Q�#n�R�ܸ���T�Vp��ogT��Q�)moIԜj���+|�u�������Q"��=~Q5'�Mn������ �u�l���C�+ t ��5!B���7 �[��/�K��a�tFW�te������=:;@݀�gN�9�&9,;��"�W�uB��7 `&�� �M�Iq{la`����j-%����L�ܳ����f��x�����&X�I�Fp)D[]���U�XV�б],ޞa%��I5di/,fqI�'9@�}��K�8����O��f#�A�����{�g4�.���mæi�>f�F�-��ɚD��FUҨ���mH��|I�h�Ͻ���x����C�@�,��&&$8�*4̆�}^Hz ���Ic�p�/�\� There is no substantial analysis performed on the Shear distributions for USP 25, the rotating disc. 2007-06-11T14:04:15+02:00 ���)ʥ��>ݽs�pvu�,���r��n ��C�ia7Y4��H��PNgM�l���>[�l}")��N�ٖ��Җ�f ��Sn��n��Rq*��� ]���vA�,���%zlՔi�V�Y�(ʸ��&��͖�ӵݼ�x��M)vsJ{�Dx��B�k���H"��` �F��_. 12 0 obj<>/ColorSpace<>/Font<>/ProcSet[/PDF/Text/ImageC/ImageI]/ExtGState<>>> endobj The approximate solubility of the articles of the Pharmacopoeia are given here primarily as information; they are not meant to be applied as tests for identifying materials.

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